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浦江LECO844分析仪

来源: 发布时间:2023年02月24日

Procedure-SolidSamplesInstrumentcalibration/driftcorrection.Addapproximately0.05gof***GraphitePowdertoa***GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.Repeatsteps3bthrough3jaminimumofthreetimesforeachcalibration/driftstandardused.Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.上海禹重实业有限公司分析仪获得众多用户的认可。浦江LECO844分析仪

浦江LECO844分析仪,分析仪

Procedure-SolidSamplesInstrumentcalibration/driftcorrection.Placethecalibration/driftstandardina***NickelBasket,andifapplicable,placethesampleintotheappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.Note:samplesusingautomationshouldbeplacedintheappropriateautoloaderpositionbeforestartingtheanalysissequence.Oncethesequencehasstarted,theautomaticanalysiswillstartandendautomatically.浦江LECO844分析仪上海禹重实业有限公司是一家专业提供分析仪的公司,欢迎您的来电!

浦江LECO844分析仪,分析仪

SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.

Instrumentcalibration/driftcorrection.a.Loginaminimumof3Standardreplicates.b.Weigha~1.000gramofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.c.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.d.Placethecalibration/driftstandardintotheopenportatthetopoftheloadinghead.e.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.上海禹重实业有限公司致力于提供分析仪,有需要可以联系我司哦!

浦江LECO844分析仪,分析仪

氧氮氢分析仪氧氮氢分析仪是一种用于材料科学领域的仪器,于2016年03月09日启用。技术指标测量范围:ON低氧0.0-300ppmOH低氧0.0-300ppm高氧0.0-2%高氧0.0-2%低氮0.0―300ppm低氢0.0-50ppm高氮0.0-2%高氢0.0-1000ppm灵敏度:氧0.01ppm;氮0.1ppm;氢0.01ppm。主要功能该仪器配置有16位微处理器和两个的分别检测高氧和低氧的红外检测池。氮和氢通过双重范围的热导检测池测量。分析过程中可自动实现从低范围到高范围的切换。样品在高功率脉冲炉的石墨坩埚中加热可达3000℃以上高温,脉冲炉采用循环水冷却。该仪器具有灵敏度高、性能好、测量范围宽和分析结果准确可靠等优点。ONH-2000氧氮氢分析仪是为快速、准确测定铜、钢、铸铁、合金、钛、镍、钼、锆、陶瓷和其它无机材料中氧、氮、氢的含量而专门设计制造的。上海禹重实业有限公司致力于提供分析仪,竭诚为您服务。浦江LECO844分析仪

上海禹重实业有限公司是一家专业提供分析仪的公司,欢迎新老客户来电!浦江LECO844分析仪

SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.浦江LECO844分析仪

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